Journal
JOURNAL OF SEPARATION SCIENCE
Volume 29, Issue 10, Pages 1344-1352Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.200600114
Keywords
capillary electrochromatography; enantiomeric separation; modified cyclodextrins; monolith; sol-gel
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The access to CD-modified monoliths for enantiomeric separation by CEC can be divided into two main approaches. (i) Silica-based monoliths, prepared by either a sol-gel process or by sintering of silica particles, are modified after fabrication by coating with a CD selector. Alternatively the fusion of CD functionalized silica particle via gluing is feasible. (ii) Rigid or homogeneous organic polymer-based monoliths, prepared by polymerization of organic monomers in the presence of a porogen, are modified with the CD selector either by copolymerization or by physical incorporation into the continuous bed.
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