Journal
CHEMISTRY LETTERS
Volume 35, Issue 7, Pages 758-759Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.2006.758
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We have developed the double ortho-lithiation of a (diethylamino)diphenylphosphine oxide and tert-butyldiphenylphosphine oxide. The resulting doubly lithiated species can be converted to various ortho-difunctionalized products as well as phosphorus heterocycles, such as dibenzophospholes and 9-phospha-10-metalla-9,10-dihydroanthracene derivatives. The structure and photophysical properties of the prepared 9-phospha-10-sila-9,10-dihydroanthracene derivative were also studied.
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