Journal
TALANTA
Volume 69, Issue 5, Pages 1072-1078Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.talanta.2005.11.023
Keywords
laser induced break down spectroscopy (LIBS); analysis of solid crude oil waste; continuous emissions monitoring; environmental impacts of trace metals; trace metals detection; LIBS applications
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Laser induced breakdown spectroscopy (LIBS) was applied for the elemental analysis of Arabian crude oil residue samples. The spectra due to trace elements such as Ca, Fe, Mg, Cu, Zn, Na, Ni, K and Mo were recorded using this technique. The dependence of time delay and laser beam energy on the elemental spectra was also investigated. Prior to quantitative analysis, the LIBS system was calibrated using standard samples containing these trace elements. The results achieved through this method were compared with conventional technique like inductively coupled plasma. (c) 2006 Elsevier B.V. All rights reserved.
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