Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 71, Issue 15, Pages 5819-5821Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo060805a
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An environmentally benign and highly efficient procedure has been developed for the direct one-pot synthesis of beta-hydroxysulfides in good yields under neutral conditions from alkenes and thiophenols in the presence of aerial oxygen using beta-cyclodextrin in water. This protocol tolerates a wide variety of functional groups or substrates and does not require the use of either acid or base catalysts. beta-Cyclodextrin can be recovered and reused for a number of runs without any loss of activity.
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