Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 10, Issue 4, Pages 833-837Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op0600613
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Representative Suzuki couplings in water using low catalyst concentrations in conjunction with microwave heating have been transferred from sealed-vessel to open-vessel reaction conditions. They have then been scaled-up to the mole scale using a dedicated multimode microwave apparatus. The reactions are complete within 20 min of heating at reflux.
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