Journal
BIOORGANIC CHEMISTRY
Volume 34, Issue 4, Pages 167-172Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.bioorg.2006.05.003
Keywords
Mannich type reaction; thiophosphate-phosphonate derivatives; acetyl chloride; X-ray crystal structure
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An improved method for the synthesis of Diphenyl alpha-(diethoxythiophosphorylamino)methylphosphonates under mild conditions is described. It consists of the reaction of diethyl thiophosphoramidate (1) with triphenyl phosphite (3) and a substituted benzylaldehyde or ketone (2) by a one-pot procedure with the aid of acetyl chloride. (c) 2006 Elsevier Inc. All rights reserved.
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