Journal
TETRAHEDRON
Volume 62, Issue 33, Pages 7738-7743Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2006.05.070
Keywords
oxazinins; adriatic shellfish; natural products; synthetic models; Mytilus galloprovincialis; NMR spectroscopy
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The analysis of a batch of toxic mussels (Mytilus galloprovincialis) from the Northern Adriatic Sea led to the isolation of a novel oxazinin, oxazinin-4. Its structure including the relative stereochemistry has been elucidated through extensive NMR analysis. A synthetic route to oxazinins has been crucial in establishing the absolute stereochemistry of oxazinin-4 and for reassigning the absolute C-2 configuration of oxazinin-1 and -2 previously isolated from toxic shellfish and stereostructurally characterized. (c) 2006 Elsevier Ltd. All rights reserved.
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