Journal
ORGANIC LETTERS
Volume 8, Issue 17, Pages 3741-3744Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol061303m
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A new electrophilic amination reaction of functionalized arylazo tosylates with alkylzinc halides or dialkylzinc reagents in THF leads to the corresponding hydrazines. A facile cleavage of the N-N bond is achieved using Raney nickel in refluxing ethanol, leading to substituted secondary aryl-alkylamines in 45-79% yield.
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