Journal
PHYSICAL CHEMISTRY CHEMICAL PHYSICS
Volume 8, Issue 31, Pages 3623-3626Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b606933a
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A layered structure of water molecules formed on a Cu(I I I) electrode surface during hydrogen evolution in sulfuric acid solution was studied by surface X-ray diffraction and infrared reflection absorption methods. Water molecules in the surface layers take a closest pack-like stacking structure with nearest-neighbor oxygen-oxygen distances in intra-(0.322(5) nm) and inter-(0.275(15) nm) layers of multi-domains; the infrared spectra of the layered water on the Cu electrode surface showed the existence of free OH(OD) and hydrogen-bonded OH(OD) of water molecule.
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