Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2006, Issue 17, Pages 3910-3916Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.200600321
Keywords
ethynyl(iodo)azulenes; oligoazulenes; oxidative coupling; cross-coupling
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The new oligoazulenes 10-14 with mixed ethynyl and butadiynyl bridges were synthesized by oxidative Eglinton coupling from the readily accessible ethynylazulenes 3, 4, 7, 9 and 15 as well as by Pd/Cu-catalyzed cross-coupling reactions with the appropriate iodoazulenes 5, 6 and 8. (c) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2006.
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