Journal
ORGANIC LETTERS
Volume 8, Issue 18, Pages 3903-3906Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol061318k
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An improved protocol for N-acetyl enamine formation is disclosed which involves LiBr-mediated addition of MeLi to substituted nitriles. The resulting enamides are isolated in high yields and excellent purity which permits subsequent hydrogenation at very low catalyst loading.
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