Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 71, Issue 18, Pages 7063-7066Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo061195h
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Microwave dielectric heating proved to be an efficient method for the one-pot and stepwise syntheses of symmetrical and unsymmetrical naphthalenediimide derivatives of alpha-amino acids. Acid-labile side chain protecting groups are stable under the reaction conditions; protection of the alpha-carboxylic group is not required. The stepwise condensation of different amino acids resulted in high yields of unsymmetrical naphthalenediimides. The reaction proceeds without racemization and is essentially quantitative.
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