Journal
ADVANCED FUNCTIONAL MATERIALS
Volume 16, Issue 14, Pages 1823-1831Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adfm.200500695
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A polyoxometalate-modified titania hybrid electrode with a tailored microstructure is studied for its photoelectrochemical applications. A highly ordered TiO2 nanotube array is prepared by low-voltage anodization followed by calcination. Functionalized polyoxophosphotungstate-titania/titanium (POW-TiO2/Ti) hybrid electrodes are synthesized by encapsulating POW nanoaggregates in the TiO2 nanotube array. The morphological characteristics and structures of POW-TiO2 composites are examined by field-emission scanning electron microscopy, X-ray diffraction, energy dispersive X-ray spectroscopy, and Fourier transform IR spectroscopy. The photoelectrochemical properties of the POW-TiO2/Ti electrodes are investigated by anodic polarization photocurrent-response measurements. Photocatalytic/photoelectrocatalytic reactivities of microstructured and nanotubular POW-TiO2/Ti photoanodes are studied for their use in the degradation of recalcitrant organic pollutants.
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