Journal
TETRAHEDRON LETTERS
Volume 47, Issue 39, Pages 6993-6995Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2006.07.123
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One-pot, waste-free oxidation of glycerol to 1,3-dihydroxyacetone (DHA) was achieved by simply applying a small electric potential (I. I V vs Ag/AgCl) to a glycerol solution in water buffered at pH 9.1 in the presence of 15 mol% TEMPO (2,2,6,6tetramethylpiperidine-l-oxyl). Prolonging the reaction time affords comparable amounts of hydroxypyruvic acid. (c) 2006 Elsevier Ltd. All rights reserved.
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