Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 71, Issue 22, Pages 8661-8664Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo0614543
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The synthesis of naturally occurring D-erythro-sphingosine and synthetically useful D-erythro-2-azidosphingosine from commercially available D-ribo-phytosphingosine is described. An important feature of this synthesis is the selective transformation of the 3,4-vicinal diol of phytosphingosine into the characteristic E-allylic alcohol of sphingosine via a cyclic sulfate intermediate.
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