Journal
INTERNATIONAL JOURNAL OF POLYMER ANALYSIS AND CHARACTERIZATION
Volume 20, Issue 4, Pages 330-343Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/1023666X.2015.1017792
Keywords
Pongamia oil; Polyesteramide; Ethylene glycol tetraacetic acid
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Funding
- King Saud University, Deanship of Scientific Research, College of Science
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In this study, ethylene glycol polyesteramide (Eg-PEA) was synthesized from N,N-bis (2-hydroxy ethyl) pongamia oil fatty amide and ethylene glycol tetraacetic acid (EGTA) through condensation polymerization. It was further modified by toluene 2,4-diisocynate in different wt.% (20, 25, 30, and 35) to obtain urethane-modified polyesteramide (Eg-UPEA). The synthesized resins were characterized using FT-IR, H-1 NMR, and C-13 NMR spectroscopic techniques, and molecular weight was determined by gel permeation chromatography (GPC). Physico-chemical and physico-mechanical analyses were carried out by standard laboratory methods. Thermal studies of Eg-UPEA were undertaken by thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) techniques. To evaluate corrosion prevention performance Eg-UPEA-coated mild steel strips were investigated by potentiodynamic polarization in different corrosive media (5wt.% NaCl, 3wt.% HCL, 2.5wt.% NaOH, and tap water) at room temperature. Thermal analysis revealed that Eg-UPEA30 may find application as an environmentally friendly corrosion protective coating and may be safely used up to 250 degrees C.
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