Journal
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
Volume 435, Issue -, Pages 172-180Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2006.07.084
Keywords
selective laser sintering; nylon 12; crystal structure; microstructure; molecular weight
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There currently exists the requirement to improve reproducibility and mechanical properties of SLS Nylon parts for rapid manufacturing (RM). In order to achieve this, further fundamental research is needed and this paper addresses this need by investigating effects of potential sources of the lack of reproducibility and reports effects in relation to crystal structure, microstructure, chemical structure (molecular weight) and mechanical properties. Different gamma crystal forms were identified and related to the unmolten particle cores and the melted/crystallised regions of the microstructure. The melt point of the gamma-form varied depending on processing conditions. Observable differences were also present when comparing the microstructure of the parts. Molecular weight of parts was significantly higher than virgin powder but used powder also showed an increase in molecular weight. This was related to improved elongation at break of parts built from the used powder, consistent with previous studies. Tensile strength showed some increase with machine parameters selected for improved strength but Young's modulus values were broadly similar. (c) 2006 Elsevier B.V. All rights reserved.
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