Journal
ORGANIC LETTERS
Volume 8, Issue 23, Pages 5275-5277Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0620141
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A highly efficient and simple synthesis of dithiocarbamates is possible based on the one-pot reaction of amines, CS2, and alkyl halides without using a catalyst under solvent-free conditions. The mild reaction conditions, high yields, and broad scope of the reaction illustrate the good synthetic utility of this method. The reaction is a highly atom-economic process for production of S-alkyl thiocarbamates and successfully can be used in high quantities in the pharmaceutical or agrochemical industries.
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