Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 10, Issue 6, Pages 1292-1295Publisher
AMER CHEMICAL SOC
DOI: 10.1021/op068011l
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The safe handling of borane complexes and alkylboranes (trialkylboranes, dialkylboranes, and trialkylborohydride reagents) and related workup issues are addressed. Oxidation of alkylboranes and quenching of reaction mixtures to safely decompose the reagent or products are discussed. Several case studies demonstrate large-scale applications of borane reagents for carboxylic acid reduction, reductive amination, and hydroboration followed by oxidation.
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