Journal
SOLID STATE IONICS
Volume 177, Issue 37-38, Pages 3333-3338Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.ssi.2006.08.032
Keywords
niobium oxide thin films; spray pyrolysis technique; scanning electron microscopy (SEM); X-ray diffraction
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Niobium oxide thin films were deposited on the glass and fluorine-doped tin oxide (FTO)-coated glass substrates using simple and inexpensive spray pyrolysis technique. Various preparative parameters like nozzle to substrate distance, spray rate, concentration of sprayed solution were optimized to obtain good substrate-adherent and transparent films. Morphological and structural characterizations of the films were carried out using scanning electron microscopy and X-ray diffraction techniques. Electrochemical characterization of the mobium oxide thin films was carried out using cyclic-voltammetry, chronoamperometry and chronocoulometry. (c) 2006 Elsevier B.V. All rights reserved.
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