Journal
MATERIALS CHEMISTRY AND PHYSICS
Volume 100, Issue 2-3, Pages 351-354Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.matchemphys.2006.01.012
Keywords
inorganic compounds; nanostructure; chemical synthesis; microstructure
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Single crystalline beta-PbO nanorods with diameter range from 40 to 120 nm and length up to 500 nm have been synthesized via a facile hydrothermal method in the presence of citrate. X-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution transmission electro-microscope (HRTEM) and SAED were used to characterize the as-obtained samples. An interesting intermediate state of self-assembled beta-PbO rod-like nanoparticles was found and the possible formation mechanism of single crystalline beta-PbO nanorods was also discussed. (c) 2006 Elsevier B.V. All rights reserved.
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