Journal
TETRAHEDRON-ASYMMETRY
Volume 17, Issue 23, Pages 3244-3247Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetasy.2006.11.032
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An oxazaborolidine catalyst is readily prepared in situ at 25 degrees C in THF using (S)-alpha,alpha-diphenylpyrrolidinemethanol and borane generated from tetrabutylammonium borohydride/CH3I reagent system. The oxazaborolidine/BH3 reagent system prepared in this way is useful for the reduction of prochiral ketones to the corresponding alcohols with up to 99% ee. (c) 2006 Elsevier Ltd. All rights reserved.
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