Journal
SYNTHESIS-STUTTGART
Volume -, Issue 24, Pages 4143-4150Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2006-950362
Keywords
carbinamines; carbinamides; organocerium reagents; non-cryogenic conditions; reaction optimization
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Subjection of methyl or n-butyllithium to a mixture of nitriles and activated cerium chloride in THF at -10 to 0 degrees C afforded the corresponding carbinamines, which were isolated as either the hydrochloride salts or acetamide or benzamide derivatives in 309 91% yields.
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