4.7 Article

Solvent effect in a solvent free reaction

Journal

CRYSTENGCOMM
Volume 9, Issue 10, Pages 879-881

Publisher

ROYAL SOC CHEMISTRY
DOI: 10.1039/b711983f

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Vapour digestion of a mixture of solid [Fe(eta(5)-C5H4-C5H4N)(2)] and solid pimelic acid HOOC(CH2)(5)COOH in the presence of solvent vapours generates co-crystals of different stoichiometry depending on the protic or aprotic nature of the solvent. The nature of the products has been ascertained by a combined use of SSNMR and X-ray diffraction.

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