Journal
TETRAHEDRON LETTERS
Volume 48, Issue 2, Pages 189-192Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2006.11.068
Keywords
trifluoromethyl ketones; carboxylic acids; trifluoroacetic anhydride; decarboxylation
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Primary and secondary carboxylic acids were converted in one step to the corresponding trifluoromethyl ketones by treatment with trifluoroacetic anhydride (TFAA) and pyridine in toluene at 60-100 degrees C followed by hydrolysis/decarboxylation with water at 45 degrees C. (c) 2006 Elsevier Ltd. All rights reserved.
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