Journal
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
Volume 53, Issue 14, Pages 3667-3670Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201311254
Keywords
hydrothermal synthesis; nanoparticles; pair distribution functions; powder X-ray diffraction; tungsten
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Funding
- Danish National Research Foundation [DNRF93]
- Danish Research Council for Nature and Universe (Danscatt)
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Pair distribution function analysis of in situ total scattering data recorded during formation of WO3 nanocrystals under hydrothermal conditions reveal that a complex precursor structure exists in solution. The WO6 polyhedra of the precursor cluster undergo reorientation before forming the nanocrystal. This reorientation is the critical element in the formation of different hexagonal polymporphs of WO3.
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