Journal
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
Volume 53, Issue 35, Pages 9380-9383Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201403213
Keywords
arynes; azaborines; azides; reactive intermediates; thermolysis
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Funding
- DFG
- Fonds der Chemischen Industrie
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Thermolysis of 9-azido-9-borafluorene in heptane solution produces the tetramer of a BN-phenanthryne. The isolation of the self-trapping product provides evidence for the involvement of the BN-aryne in the thermolysis reaction. Its formation may be rationalized by denitrogenation of the azide and ring enlargement.
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