Journal
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
Volume 54, Issue 3, Pages 888-891Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201409860
Keywords
C-H activation; olefination; palladium; phenylacetic acid; template synthesis
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Funding
- Scripps Research Institute
- U.S. NSF [CHE-1011898]
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meta-C-H olefination of phenylacetic acid derivatives has been achieved using a commercially available nitrile-containing template. The identification of N-formyl-protected glycine as the ligand (Formyl-Gly-OH) was crucial for the development of this reaction. Versatility of the template approach in accommodating macrocyclopalladation processes with different ring sizes is demonstrated.
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