Journal
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
Volume 53, Issue 39, Pages 10495-10499Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201406479
Keywords
C-N bond formation; cyclization; dehydrogenative coupling; imines; nitrogen oxides
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Funding
- National Natural Science Foundation of China [21325206, 21172006]
- National Young Top-notch Talent Support Program
- Ph.D. Programs Foundation of the Ministry of Education of China [20120001110013]
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An efficient method for the synthesis of quinoxaline N-oxides proceeds by the dehydrogenative N-incorporation of simple imines by C(sp(2))-H and C(sp(3))-H bond functionalization. The overall transformation involves the cleavage of three C H bonds. The reaction is easily handled and proceeds under mild conditions. Simple and readily available tert-butyl nitrite (TBN) was employed as the NO source.
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