Journal
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
Volume 53, Issue 38, Pages 10213-10217Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201404692
Keywords
alkynes; arynes; carbon dioxide; copper; multicomponent reactions
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Funding
- Japan Society for the Promotion of Science (JSPS)
- Global COE Program (Chemistry Innovation through Cooperation of Science and Engineering)
- University of Tokyo
- Ministry of Education, Culture, Sports, Science and Technology (MEXT) (Japan)
- Japan Science and Technology Agency (JST)
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A copper-catalyzed multicomponent coupling reaction between in situ generated ortho-arynes, terminal alkynes, and carbon dioxide was developed to access isocoumarins in moderate to good yields. The key to this CO2-incorporating reaction was the use of a versatile N-heterocyclic carbene/copper complex that was able to catalyze multiple transformations within the three-component reaction.
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