4.6 Article

Trichloroisocyanuric acid (TCCA) as a mild and efficient catalyst for the trimethylsilylation of alcohols and phenols with hexamethyldisilazane (HMDS) under heterogonous conditions

Journal

CATALYSIS COMMUNICATIONS
Volume 8, Issue 3, Pages 543-547

Publisher

ELSEVIER SCIENCE BV
DOI: 10.1016/j.catcom.2006.06.018

Keywords

alcohols; phenols; trichloroisocyanuric acid; hexamethyldisilazane; trimethylsilylation

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A novel and efficient method for the trimethylsilylation of various alcohols and phenols with hexamethyldisilazane (HMDS) catalyzed by trichloroisocyanuric acid (TCCA) in good to excellent yields in dichloromethane at room temperature was described. (c) 2006 Elsevier B.V. All rights reserved.

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