Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 72, Issue 6, Pages 2106-2117Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo0624389
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A comprehensive study of a general and effective one-step procedure for the synthesis of beta-sulfonamidodisulfides directly from N-tosyl aziridines in a regio- and stereospecific manner under neutral conditions without the use of any Lewis acid or base has been reported. This methodology is extended to the synthesis of an optically pure cyclic seven-membered disulfide 29. Synthesis of a variety of beta-sulfonamidosulfides involving tandem, multistep reactions in one pot is also reported.
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