Journal
TETRAHEDRON-ASYMMETRY
Volume 18, Issue 5, Pages 671-678Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetasy.2007.03.004
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This paper describes the establishment of a new synthetic route to the hydrobromide salt of (+)-coniceine 1 with high enantiopurity in five steps and 8% overall yield. The key step is the reductive photocyclization of an acyclic chiral dienamide, for which a convenient one-pot synthesis is described. (c) 2007 Published by Elsevier Ltd.
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