Journal
SYNLETT
Volume -, Issue 6, Pages 897-900Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2007-970785
Keywords
palladium; Heck reaction; polycyclic aromatic; hydrocarbons; annulated cyclopentadienes
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A bisnaphthyl-substituted acenaphthylene is synthesized via two independent two-step procedures, Pd-catalyzed and classically with Grignard reagents. The subsequent dehydrocyclization stops after the first carbon-carbon bond formation, leading to an octacyclic pi-system as the main product.
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