Journal
ORGANIC LETTERS
Volume 9, Issue 8, Pages 1577-1580Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol070429w
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[GRAPHICS] Reaction of a ketocalixarene with 2.2 equiv or an excess of PhLi affords diaddition and tetraaddition products, respectively. Ionic hydrogenation of the tetraalcohol 8a yields a calix[4]arene monosubstituted by phenyl groups at all four methylene bridges.
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