Journal
JOURNAL OF CHROMATOGRAPHY A
Volume 1147, Issue 1, Pages 37-41Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.chroma.2007.02.023
Keywords
carrageenan; LC-MS; electrospary ionisation; porous graphitic carbon
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Enzymatically digested oligosaccharides of K-carrageenans were separated on a porous graphitic carbon (PGC) column and characterised on-line by electrospray ionisation mass spectrometry (ESI-MS). Two different developing ions were applied. Among them ammonium hydrogencarbonate showed more eluting power as it should on normal anion-exchange stationary phases. The oligosaccharides were detected by ESI-MS as fully deprotonated oligosaccharides. (c) 2007 Elsevier B.V. All rights reserved.
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