Journal
POLYMER
Volume 48, Issue 9, Pages 2489-2495Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.polymer.2007.02.032
Keywords
atom transfer radical polymerization; anionic polymerization; H-shaped block copolymer
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A novel fluorescent dye labeled H-shaped block copolymer, (PMMA-Fluor-PS)(2)-PEO-(PS-Fluor-PMMA)(2), is synthesized by the combination of atom transfer radical polymerization (ATRP) and anionic polymerization (AP). To obtain the designated structure of the copolymer, a macroinitiator, 2,2-dichloro acetyl-PEO-2,2-dichloro acetyl (DCA-PEO-DCA), was prepared from DCAC and poly(ethylene oxide). The copolymer was characterized by H-1 NMR, GPC and fluorescence spectroscopy. (c) 2007 Elsevier Ltd. All rights reserved.
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