Journal
ORGANIC LETTERS
Volume 9, Issue 9, Pages 1695-1698Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0703940
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Olefin cross-metathesis between alpha-methylene-gamma-butyrolactone and terminal olefins is described. Moderate to excellent yields of alpha-alkylidene-gamma-butyrolactones were obtained with high E-stereoselectivity in the presence of low catalyst loading in refluxing CH2Cl2. In addition, the use of various additives was found to have a dramatic effect on the efficiency of the cross-metathesis (CM) process by circumventing the formation of the isomerized byproduct.
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