Journal
TETRAHEDRON
Volume 63, Issue 18, Pages 3826-3839Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2007.02.038
Keywords
chlorin; hydroporphyrin; hydrodipyrrin; dipyrromethane
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Funding
- NIGMS NIH HHS [R01 GM036238, R01 GM036238-20, R01 GM036238-18, R01 GM036238-19] Funding Source: Medline
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Five routes to stable chlorins bearing 0 or 1 meso substituents have been investigated, among which reaction of a 9-bromo-1-formyldipyrromethane and 2,3,4,5-tetrahydro-1,3,3-trimethyldipyrrin proved most effective. Application of this route afforded metallochlorins [Cu(II), Zn(II)), and Pd(Il)] including the chlorin lacking any beta-pyrrole and meso substituents. (C) 2007 Elsevier Ltd. All rights reserved.
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