4.7 Article

Lead-free SrBi4Ti4O15 and Bi4Ti3O12 material fabrication using the microwave-assisted molten salt synthesis method

Journal

JOURNAL OF THE AMERICAN CERAMIC SOCIETY
Volume 90, Issue 5, Pages 1659-1662

Publisher

WILEY
DOI: 10.1111/j.1551-2916.2007.01632.x

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In this paper, the microwave-assisted molten salt method (MAMSS) and molten salt method (MSS) were used to synthesize SrBi4Ti4O15 (SBT). The phase constitution was determined by powder X-ray diffraction and the microstructure of powder was examined by scanning electron microscopy. In contrast to the conventional MSS method, MAMSS produces more distinct plate-like grains and synthesizes both SBT and Bi4Ti3O12 (BTO) at 600 degrees C with a 30-min soaking time. The increase of temperature and soaking time can make the plate-like grains of BTO more distinct.

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