Journal
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS
Volume 68, Issue 5-6, Pages 1203-1206Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.jpcs.2007.03.027
Keywords
inorganic compounds; chemical synthesis; X-ray diffraction; electrochemical properties
Funding
- Korea Institute of Industrial Technology(KITECH) [10028363] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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The LiMnPO4 fine particles were synthesized by polyol method. To optimize the synthesis conditions of the LiMnPO4 compounds, we have prepared the LiMnPO4 compound with different processing conditions. The samples were characterized by X-ray diffraction, scanning electron microscope observation and infrared spectroscope study. The particle size of the as-prepared samples are very small than the sample calcined at 500 degrees C for 3 h in Ar. The electrochemical properties of the cathodes were studied by galvanostatic method. All the samples exhibit a sloping line of the voltage profile, which is the characteristic of the nanoparticles. (c) 2007 Elsevier Ltd. All rights reserved.
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