Journal
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL
Volume 268, Issue 1-2, Pages 65-69Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.molcata.2006.12.004
Keywords
bis(oxazoles); pincer ligands; Suzuki-Miyaura cross coupling; palladium; biaryls
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Introducing bis(oxazole) ligands to catalysis: novel bis(oxazole) ligands could be readily synthesized from isophthaloyl dichlorides and ethyl glycinate hydrochlorides or 6-aminoacetophenone hydrochloride. Their corresponding pincer palladium complexes proved to be extremely robust catalysts for Suzuki-Miyaura cross coupling reactions, allowing the synthesis of biaryls under aerobic conditions with turn over numbers of up to 790,000 and turn over frequencies of up to 49,000h(-1). (c) 2007 Elsevier B.V. All rights reserved.
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