Journal
ANALYTICAL METHODS
Volume 6, Issue 12, Pages 4396-4401Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4ay00666f
Keywords
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Funding
- High Impact Research from the Ministry of Higher Education (MOHE) Malaysia [UM.C/HIR/MOHE/ENG/44]
- [UM.TNC2/IPPP/UPGP/Geran (PPP)/PV012/2011A]
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Precise and accurate porosity measurement is essential for characterization of porous materials. Considering Archimedes' principle based liquid displacement methods of measuring porosity we have developed an excellent modified micro-volumetric method of porosity measurement. Changes in the liquid level in a glass pipette after immersing and also removing the porous sample were recorded by using a digital camera and analysed by ImageJ (R) software. Results of porosity measurement through a micro-volumetric method were compared with micro-CT results. Bland-Altman analysis showed a much higher precision and accuracy for our micro-volumetric method (bias = -0.023, Cl: ] -0.459, 0.413[, SD = 1.96 O') compared to the micro-CT method (bias = 6.075, Cl: ] -20.993, 33.142[, SD = 1.96 O'). Our highly precise and accurate micro-volumetric method of porosity measurement is particularly applicable to small ultra-light highly porous materials.
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