Journal
ANALYTICAL METHODS
Volume 5, Issue 22, Pages 6360-6367Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3ay41170b
Keywords
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Funding
- National Natural Science Foundation of China [21065005, 21165010, 21101146]
- Young Scientist Foundation of Jiangxi Province [20112BCB23006, 20122BCB23013]
- Foundation of Jiangxi Educational Committee [GJJ13243, GJJ13244]
- State Key Laboratory of Electroanalytical Chemistry [SKLEAC201310]
- State Education Ministry
- Key Laboratory of Functional Small Organic Molecules [KLFS-KF-201214, KLFS-KF-01218]
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Hierarchical Cu-Co-Ni nanostructures (Cu-Co-Ni NSs) attached to carbon nanofibers (CNFs) modified glassy carbon electrode (GCE) was prepared by electrodeposition. Scanning electron microscopy results indicated that many hierarchical Cu-Co-Ni NSs were formed and uniformly dispersed on the CNFs/GCE surface. The electrochemical behavior and electrocatalytic performance of the Cu-Co-Ni NSs/CNFs/GCE towards the oxidation of glucose were evaluated by cyclic voltammograms, chronoamperometry and amperometric methods. The results revealed that Cu-Co-Ni NSs/CNFs/GCE has a good electrocatalytic activity for glucose oxidation and could be used as a nonenzymatic glucose sensor. The sensor showed an acceptable linear range from 0.01 to 4.30 mM with a sensitivity of 104.68 mu A mM cm(-2), and a detection limit of 3.05 mM (S/N = 3). The good catalytic activity, high sensitivity, good selectivity and stability rendered the Cu-Co-Ni NSs/CNFs/GCE to be a promising electrode for constructing a nonenzymatic glucose sensor.
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