Journal
TETRAHEDRON LETTERS
Volume 48, Issue 24, Pages 4229-4233Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2007.04.075
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Total synthesis of (+/-)-thallusin was achieved using Hg(OTf)(2)-PhNMe2-induced olefin cyclization, and Suzuki coupling with a pyridyllboronic acid derivative. Hg(OTf)(2) also acted as a catalyst to isomerize the double bond into the more thermodynamically stable isomer when treated in toluene. Synthetic (+/-)-thallusin as well as an analogue showed morphogenesis-inducing activity. (c) 2007 Elsevier Ltd. All rights reserved.
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