Journal
ANALYTICA CHIMICA ACTA
Volume 593, Issue 1, Pages 98-102Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.aca.2007.04.038
Keywords
synephrine; biogenic amines; adrenergic amines; herbal extracts; dietary supplements; monolithic column chromatography; acidic potassium permanganate chemiluminescence
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Adrenergic amines found in extracts of Citrus aurantium (bitter orange) evoke analytically useful chemiluminescence with acidic potassium permanganate in the presence of polyphosphates. From corrected chemiluminescence spectra, the wavelength of maximum intensity for these reactions was 680 +/- 5 nm and, using flow injection analysis methodology, limits of detection for synephrine, octoparnine, tyramine and hordenine were found to be between 1 x 10(-9) and 1 x 10(-8) M. We have applied this method of detection to the rapid determination of synephrine in dietary supplements using monolithic column chromatography. (c) 2007 Elsevier B.V. All rights reserved.
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