Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 72, Issue 13, Pages 4611-4620Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo062423a
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Funding
- NIGMS NIH HHS [GM-29028] Funding Source: Medline
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A second-generation strategy for construction of (+)-nodulisporic acids A and B based on the development of a new, effective modular indole synthesis exploiting a sequential Stille cross-coupling/Buchwald-Hartwig union/cyclization tactic is disclosed. This strategy evolved due to the considerable acid instability of the C(24) hydroxyl group observed in several advanced intermediates during our first-generation approach.
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