Journal
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY
Volume 43, Issue 7, Pages 1058-1064Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S1070428007070202
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A simple and effective synthesis of 3,4-dihydropyrimidin-2(1H)-one and 3,4-dihydropyrimidine-2(1H)-thione derivatives has been developed on the basis of three-component condensation of substituted aromatic and heterocyclic aldehydes, methyl acetoacetate, and urea or thiourea in the presence of 10% of an acidic task-specific ionic liquid ([C(4)mim][HSO4]) as catalyst under microwave irradiation in the absence of a solvent. The proposed procedure ensures short reaction times (4.4-8 min) and good yields after purification by recrystallization.
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