Journal
JOURNAL OF FLUORINE CHEMISTRY
Volume 128, Issue 7, Pages 851-856Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2007.04.012
Keywords
trihalomethyl sulfides; trifluoromethyl sulfones; trifluoromethanesulfinates; trifluoromethylation; halogen exchange; alkyl thiocyanates; beta-elimination
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Trifluoromethanesulfinate (triflinate) salts can be prepared in an ecofriendly way by beta-elimination of aliphatic triflones bearing an acidic hydrogen in beta position. This technique allows the synthesis of various triflinate salts under mild conditions. (c) 2006 Elsevier B.V. All rights reserved.
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