Journal
CHINESE CHEMICAL LETTERS
Volume 18, Issue 7, Pages 799-802Publisher
CHINESE CHEMICAL SOCIETY
DOI: 10.1016/j.cclet.2007.05.001
Keywords
tetrahydropyranylation; synergistic effect; copper methanesulfonate; acetic acid
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A synergistic catalytic effect between copper methanesulfonate and acetic acid in tetrahydropyranylation of alcohols and phenol at room temperature under solvent free condition has been described. Both alcohols (primary, secondary and tertiary) and phenols reacted with 3,4-dihydro-2H-pyran smoothly to afford the corresponding tetrahydropyranyl ethers in good yields. (C) 2007 Min Wang. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.
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